trideuteriomethylcyclohexanone

Base Information

• Chemical Name: trideuteriomethylcyclohexanone
• CAS No.: 56292-73-0
• Molecular Formula: C₇H₁₂O
• Molecular Weight: 115.148
• Mol file: 56292-73-0.mol

Synonyms:

Chemical Property of trideuteriomethylcyclohexanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trideuteriomethylcyclohexanone

There total 1 articles about trideuteriomethylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ trideuteriomethylcyclohexanone (56292-73-0)

Guidance literature:

Aethyl cyclohexanon-2-carboxylat 1) CD3I in NaOC2H5-Loesung 2) sd.HCl + Essigsaeure ;

DOI:10.1021/jo01341a002

Reference yield: 22.0%

trideuteriomethylcyclohexanone (56292-73-0) + Allyl chloroformate (2937-50-0) → C11H13(2)H3O3

Guidance literature:

trideuteriomethylcyclohexanone; With potassium tert-butylate; In N,N-dimethyl-formamide; for 12h;

Allyl chloroformate; In N,N-dimethyl-formamide; at 25 ℃; Cooling with ice;

DOI:10.1002/chem.201003383

Reference yield:

pyrrolidine (123-75-1) + trideuteriomethylcyclohexanone (56292-73-0) → C11H17(2)H3NO(1-)*Li(1+)

Guidance literature:

With lithium hexamethyldisilazane; In toluene; at -78 ℃; Kinetics;

DOI:10.1021/ja030582v