N-(2,4-Dichlorphenyl)-anthranilsaeurenitril

Base Information

• Chemical Name: N-(2,4-Dichlorphenyl)-anthranilsaeurenitril
• CAS No.: 13625-37-1
• Molecular Formula: C₁₃H₈Cl₂N₂
• Molecular Weight: 263.126
• Mol file: 13625-37-1.mol

Synonyms:

Chemical Property of N-(2,4-Dichlorphenyl)-anthranilsaeurenitril

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(2,4-Dichlorphenyl)-anthranilsaeurenitril

There total 4 articles about N-(2,4-Dichlorphenyl)-anthranilsaeurenitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,4-Dichlorphenyl)-anthranilsaeureamid (13625-36-0) → N-(2,4-Dichlorphenyl)-anthranilsaeurenitril (13625-37-1)

Guidance literature:

With triethylamine; trichlorophosphate;

DOI:10.1021/jm00307a025

Reference yield:

N-(2,4-dichloro-phenyl)-anthranilic acid (18201-58-6) → N-(2,4-Dichlorphenyl)-anthranilsaeurenitril (13625-37-1)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) SOCl₂, SOCl₂, DMF, (ii) aq. NH₃

2: POCl₃, Et₃N

With triethylamine; trichlorophosphate;

DOI:10.1021/jm00307a025

Reference yield:

sodium o-bromobenzoate (17264-73-2) → N-(2,4-Dichlorphenyl)-anthranilsaeurenitril (13625-37-1)

Guidance literature:

Multi-step reaction with 3 steps

1: CaH₂, CuBr₂, diglyme

2: (i) SOCl₂, SOCl₂, DMF, (ii) aq. NH₃

3: POCl₃, Et₃N

With calcium hydride; diethylene glycol dimethyl ether; triethylamine; copper(ll) bromide; trichlorophosphate;

DOI:10.1021/jm00307a025

upstream raw materials:

N-(2,4-Dichlorphenyl)-anthranilsaeureamid

N-(2,4-dichloro-phenyl)-anthranilic acid

sodium o-bromobenzoate

2,4-Dichloroaniline