Benzoic acid, 2-bromo-, sodium salt

Base Information

• Chemical Name: Benzoic acid, 2-bromo-, sodium salt
• CAS No.: 17264-73-2
• Molecular Formula: C7H5BrO2.Na
• Molecular Weight: 223.001
• Mol file: 17264-73-2.mol

Synonyms:2-Brom-benzoesaeure,Natrium-Verbindung;2-bromo-benzoic acid,sodium-compound;Na-Salz der 2-Brom-benzoesaeure;sodium o-bromobenzoate;

Chemical Property of Benzoic acid, 2-bromo-, sodium salt

Chemical Property:

• PSA: 40.13000
• LogP: 0.81260

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-bromo-, sodium salt

There total 1 articles about Benzoic acid, 2-bromo-, sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitrophenol sodium salt (824-78-2) + 2-bromobenzoic-acid (88-65-3) → 4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + sodium o-bromobenzoate (17264-73-2)

Guidance literature:

With 1-butyl-2,3-dimethylimidazolium bis-(trifluoromethanesulfonyl)amide; In methanol; at 24.84 ℃; Reagent/catalyst; Equilibrium constant;

DOI:10.1021/jo100914p

Reference yield: 85.0%

dichlorobis(η5-methylcyclopentadienyl)titanium(IV) (1282-40-2) + sodium o-bromobenzoate (17264-73-2) → bis(methylcyclopentadienyl)bis(o-bromobenzoate)titanium

Guidance literature:

In benzene; 30°C, stirring, 12 h; removing pptd. salt by filtration, concg. filtrate in vac., addn. of petroleum ether, refrigerating at 0°C overnight, washing crystals with petroleum ether; elem. anal.;

Reference yield: 84.0%

2-ethoxy-ethanol (110-80-5) + sodium o-bromobenzoate (17264-73-2) → C11H13BrO3 (1013325-36-4)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; triethylamine; In N,N-dimethyl-formamide; for 4h; Heating;

DOI:10.1016/j.tetlet.2007.12.068

upstream raw materials:

4-nitrophenol sodium salt

2-bromobenzoic-acid

Downstream raw materials:

o-cyanobenzoic acid, sodium salt

Phenacyl-o-brombenzoat

N-(2,4-dichloro-phenyl)-anthranilic acid

2-(4-chloroanilino)benzoic acid