(4-formylphenyl)diethoxylphosphine

Base Information

Chemical Name:(4-formylphenyl)diethoxylphosphine
CAS No.:1409943-07-2
Molecular Formula:C₁₁H₁₅O₃P
Molecular Weight:226.212
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-formylphenyl)diethoxylphosphine

Chemical Property:

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Technology Process of (4-formylphenyl)diethoxylphosphine

There total 2 articles about (4-formylphenyl)diethoxylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4762-34-9
diethyl (4-bromophenyl)phosphonite

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1409943-07-2
(4-formylphenyl)diethoxylphosphine

Guidance literature:: diethyl (4-bromophenyl)phosphonite; With n-butyllithium; In tetrahydrofuran; hexane; at -70 ℃; for 1h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; hexane; at 20 ℃; for 7h; Inert atmosphere;
DOI:10.1021/ic301394x

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 1409943-07-2
(4-formylphenyl)diethoxylphosphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

1.2: 8 h / 20 °C / Inert atmosphere

2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -70 °C / Inert atmosphere

2.2: 7 h / 20 °C / Inert atmosphere

With n-butyllithium; In tetrahydrofuran; hexane;
DOI:10.1021/ic301394x