N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

Base Information

Chemical Name:N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride
CAS No.:137680-56-9
Molecular Formula:C₁₃H₂₃Cl₂N₂Si₂Tl
Molecular Weight:538.799
Hs Code.:

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Chemical Property of N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

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Technology Process of N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

There total 1 articles about N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 24261-90-3
N,N,N'-tris(trimethylsilyl)benzamidine

: 13453-32-2
thallium (III) chloride

: (C₆H₅C(NHSi(CH₃)3)2)⁽¹⁺⁾*(C₆H₅C(NSi(CH₃)3)2TlCl₃)^(1-)=(C₆H₅C(NHSi(CH₃)3)2)(C₆H₅C(NSi(CH₃)3)2TlCl₃)

: 137680-56-9
N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

Guidance literature:: In tetrahydrofuran; byproducts: ClSi(CH3)3; absence of moisture, solution is stirred at room temp. and allowed to stand for 12 h; volume is reduced under vacuum, filtrate is washed with THF and dried under vacuum, elem. anal.;

Reference yield: 84.0%

: 137680-56-9
N,N'-bis(trimethylsilyl)benzamidinato thallium dichloride

: 24261-90-3
N,N,N'-tris(trimethylsilyl)benzamidine

: (C₆H₅C(NHSi(CH₃)3)2)⁽¹⁺⁾*(C₆H₅C(NSi(CH₃)3)2TlCl₃)^(1-)=(C₆H₅C(NHSi(CH₃)3)2)(C₆H₅C(NSi(CH₃)3)2TlCl₃)

Guidance literature:: In dichloromethane; absence of moisture, addn. of HCl-gas to the mixed solution at 0°C; filtrate is washed with CH2Cl2 and dried under vacuum, elem. anal.;