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2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol

Base Information Edit
  • Chemical Name:2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol
  • CAS No.:88065-34-3
  • Molecular Formula:C27H32OS2
  • Molecular Weight:436.682
  • Hs Code.:
  • Mol file:88065-34-3.mol
2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol

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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of 2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol Edit
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Technology Process of 2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol

There total 6 articles about 2-methyl-6-(p-tolyl)-3,3-bisphenylthioheptan-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 5 steps
1: 1.) sodium hydride / 1.) dimethoxyethane, 30 min, room temperature 2.) reflux, 5 h, dimethoxy ethane
2: 96 percent / hydrogen / 5percent palladium on charcoal / ethanol / 6 h / 760 Torr
3: 85 percent / lithium aluminium hydride / tetrahydrofuran / 0.5 h
4: 57 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h / other reagent
5: 1.) n-butyl-lithium, TMEDA 2.) n-butyl-lithium / 1.) hexane, THF, 0 deg C, 15 min 2.) 30 min, hexane, THF
With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen; sodium hydride; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/P19850001237
Guidance literature:
Multi-step reaction with 4 steps
1: 96 percent / hydrogen / 5percent palladium on charcoal / ethanol / 6 h / 760 Torr
2: 85 percent / lithium aluminium hydride / tetrahydrofuran / 0.5 h
3: 57 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h / other reagent
4: 1.) n-butyl-lithium, TMEDA 2.) n-butyl-lithium / 1.) hexane, THF, 0 deg C, 15 min 2.) 30 min, hexane, THF
With lithium aluminium tetrahydride; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydrogen; pyridinium chlorochromate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/P19850001237
Guidance literature:
Multi-step reaction with 2 steps
1: 57 percent / pyridinium chlorochromate / CH2Cl2 / 1.5 h / other reagent
2: 1.) n-butyl-lithium, TMEDA 2.) n-butyl-lithium / 1.) hexane, THF, 0 deg C, 15 min 2.) 30 min, hexane, THF
With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; pyridinium chlorochromate; In dichloromethane;
DOI:10.1039/P19850001237
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