P,P-Bis(2-methylphenyl)phosphinodithioic acid

Base Information

Chemical Name:P,P-Bis(2-methylphenyl)phosphinodithioic acid
CAS No.:1122052-41-8
Molecular Formula:C₁₄H₁₅PS₂
Molecular Weight:278.379
Hs Code.:
DSSTox Substance ID:DTXSID101251687
Nikkaji Number:J3.044.196F

Synonyms:SCHEMBL8491905;DTXSID101251687;1122052-41-8;P,P-Bis(2-methylphenyl)phosphinodithioic acid

Suppliers and Price of P,P-Bis(2-methylphenyl)phosphinodithioic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of P,P-Bis(2-methylphenyl)phosphinodithioic acid

Chemical Property:

XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:278.03527982
Heavy Atom Count:17
Complexity:277

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC=CC=C1P(=S)(C2=CC=CC=C2C)S

Technology Process of P,P-Bis(2-methylphenyl)phosphinodithioic acid

There total 4 articles about P,P-Bis(2-methylphenyl)phosphinodithioic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 29949-64-2
di(o-tolyl)phosphine

: 1122052-41-8
bis(o-tolyl)dithiophosphinic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfur / toluene / 3 h / Inert atmosphere; Reflux

1.2: 20 °C

2.1: hydrogenchloride / diethyl ether; water

With hydrogenchloride; sulfur; In diethyl ether; water; toluene;
DOI:10.1039/c1dt11637a

Reference yield:

: C₁₄H₁₄PS₂^(1-)*Na⁽¹⁺⁾

: 1122052-41-8
bis(o-tolyl)dithiophosphinic acid

Guidance literature:: With hydrogenchloride; In diethyl ether; water;
DOI:10.1039/c1dt11637a

Reference yield:

: 30309-80-9
di-o-tolylphosphine oxide

: 1122052-41-8
bis(o-tolyl)dithiophosphinic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride

2.1: sulfur / toluene / 3 h / Inert atmosphere; Reflux

2.2: 20 °C

3.1: hydrogenchloride / diethyl ether; water

With hydrogenchloride; diisobutylaluminium hydride; sulfur; In diethyl ether; water; toluene;
DOI:10.1039/c1dt11637a