C₂₂H₃₄NO₇P

Base Information

• Chemical Name: C₂₂H₃₄NO₇P
• CAS No.: 870544-50-6
• Molecular Formula: C₂₂H₃₄NO₇P
• Molecular Weight: 455.488
• Mol file: 870544-50-6.mol

Synonyms:

Chemical Property of C₂₂H₃₄NO₇P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₃₄NO₇P

There total 4 articles about C₂₂H₃₄NO₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methyl-2-propenoic acid 2-hydroxyethyl ester (868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5) → C22H34NO7P (870544-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: Et₃N / toluene / 4 h / 0 - 5 °C

2.1: ethanol / 2 h / 25 °C

2.2: 48 h / 23 °C

With triethylamine; In ethanol; toluene; 2.1: Michael addition;

DOI:10.1021/ma047526e

Reference yield:

ethylene glycol acrylate methacrylate (69040-48-8) + β-(N-benzyl)aminoethylphosphonic acid diethyl ester (79782-58-4) → C22H34NO7P (870544-50-6)

Guidance literature:

ethylene glycol acrylate methacrylate; β-(N-benzyl)aminoethylphosphonic acid diethyl ester; In ethanol; at 25 ℃; for 2h;

at 23 ℃; for 48h; Further stages.;

DOI:10.1021/ma047526e

Reference yield:

Diethyl vinylphosphonate (682-30-4) → C22H34NO7P (870544-50-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 24 h / 70 °C

2.1: ethanol / 2 h / 25 °C

2.2: 48 h / 23 °C

In ethanol; 1.1: Michael addition / 2.1: Michael addition;

DOI:10.1021/ma047526e

upstream raw materials:

ethylene glycol acrylate methacrylate

β-(N-benzyl)aminoethylphosphonic acid diethyl ester

2-methyl-2-propenoic acid 2-hydroxyethyl ester

Diethyl vinylphosphonate