[Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3

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Chemical Name:[Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3
CAS No.:223122-90-5
Molecular Formula:C₅₆H₅₆Cu₂N₅O₃P₄*NO₃
Molecular Weight:1160.08
Hs Code.:

Synonyms:

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Chemical Property of [Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3

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Technology Process of [Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3

There total 1 articles about [Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 12775-96-1,15158-11-9,15721-63-8,16941-75-6,17493-86-6,19498-52-3,20499-83-6,20499-84-7,20499-85-8,20499-86-9,20573-10-8,20573-11-9,21595-51-7,21595-52-8,22206-52-6,26445-28-3,28959-95-7,37362-93-9,39417-05-5,54603-16-6,54603-23-5,54603-32-6,54603-40-6,54603-48-4,54603-81-5,54603-89-3,56316-56-4,95985-91-4,122297-32-9,7440-50-8
copper

: copper(II) nitrate

: 1467-79-4
NCNMe₂

: 2071-20-7
bis-diphenylphosphinomethane

: 223122-90-5
[Cu2(bis(diphenylphosphino)methane)2(η(1)-dimethyl cyanamide)2(η(1).,μ2-ONO2)]NO3

Guidance literature:: In dichloromethane; acetonitrile; N2-atmosphere; refluxing Cu(NO3)2 with Cu powder in MeCN for 4 h, filtration, addn. of 2 equiv. of phosphine, stirring for 1 h, solvent removal (reduced pressure), dissoln. in CH2Cl2, addn. of excess of cyanamide, stirring for 30 min; concn., pptn. on addn. of petroleum ether, filtration, washing (petroleum ether), drying (vac.); elem. anal.;
DOI:10.1021/ic9801589