InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin

Base Information

• Chemical Name: InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin
• CAS No.: 690957-61-0
• Molecular Formula: C₆₀H₆₀ClInN₄
• Molecular Weight: 987.436

Synonyms:

Chemical Property of InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin

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Technology Process of InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin

There total 1 articles about InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

indium(III) chloride (10025-82-8) + copper dichloride → InCl 5,10,15,20-tetrakis(4-tert-butylphenyl)porphyrin (690957-61-0)

Guidance literature:

With catalyst: 1,8-diazabicyclo [5.4.0] undec-7-ene; In neat (no solvent); Irradiation (UV/VIS); a ligand (1.2 mmol) and InCl3 (1.79 mmol) were ground together in a quartz vessel, poured into DBU and irradiated in a microwave oven at 240 W for 5 min; the compd. was dissolved in ethanol; butyl acetate as well as petroleum ether was added for pptn.; recrystn. with methanol; column chromy. (aluminum oxide, chloroform); elem. anal.;

DOI:10.1016/j.jorganchem.2004.01.017

upstream raw materials:

indium(III) chloride

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