3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid

Base Information

• Chemical Name: 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid
• CAS No.: 116654-74-1
• Molecular Formula: C₁₃H₁₅NO₂S*ClH
• Molecular Weight: 285.795

Synonyms:

Chemical Property of 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

Ethyl2-amino-3-(1-benzothiophen-3-yl)propanoate;hydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid

There total 4 articles about 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.7%

3-thienyl-3>-2-formamidopropionsaeureethylester (117209-90-2) → 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid (116654-74-1)

Guidance literature:

With hydrogenchloride; In ethanol; Ambient temperature;

DOI:10.1002/ardp.19883210512

Reference yield:

3-chloromethylbenzothiophene (3216-47-5) → 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid (116654-74-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 48 percent / 1.) EtONa / ethanol / 1.) r.t., 10 min, 2.) reflux, 3 h

2: 53 percent / NaCl / dimethylsulfoxide; H₂O / 0.25 h / Heating

3: 86.7 percent / 3.4 N HCl / ethanol / Ambient temperature

With hydrogenchloride; sodium ethanolate; sodium chloride; In ethanol; water; dimethyl sulfoxide;

DOI:10.1002/ardp.19883210512

Reference yield:

3-thienyl-3>-(2-carbethoxy-2-formamido)-propionsaeureethylester (72071-48-8) → 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid (116654-74-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 53 percent / NaCl / dimethylsulfoxide; H₂O / 0.25 h / Heating

2: 86.7 percent / 3.4 N HCl / ethanol / Ambient temperature

With hydrogenchloride; sodium chloride; In ethanol; water; dimethyl sulfoxide;

DOI:10.1002/ardp.19883210512

upstream raw materials:

ethanol

(R)-α-amino-3-[1]benzothiophene-3-ylpropionic acid

3-thienyl-3>-2-formamidopropionsaeureethylester

3-chloromethylbenzothiophene

Downstream raw materials:

N-cyclohexyl-1,2,3,4-tetrahydro<1>benzothieno<2,3-c>pyridine-3-carboxamide hydrochloride

N-cyclohexyl-2-(tert-butoxycarbonyl)-1,2,3,4-tetrahydro<1>benzothieno<2,3-c>pyridine-3-carboxamide

2-(2-chlorobenzoyl)-1,2,3,4-tetrahydro<1>benzothieno<2,3-c>pyridine-3-carboxylic acid ethyl ester

2-Benzoyl-1,2,3,4-tetrahydro-benzo[4,5]thieno[2,3-c]pyridine-3-carboxylic acid ethyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 116654-74-1 3-thienyl-3>-2-amino-propionsaeureethylester-hydrochlorid

Send

Send

Metric Ton KG G Pound L ML

Send

Send