Technology Process of C17H23NO2
There total 3 articles about C17H23NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; palladium diacetate; diisopropylamine; triphenylphosphine;
In
ethyl acetate;
at 50 ℃;
for 5h;
DOI:10.1016/j.bmcl.2013.02.118
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / N,N-dimethyl-formamide / 15 h / 20 °C
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / 100 °C
3: palladium diacetate; triphenylphosphine; copper(l) iodide; diisopropylamine / ethyl acetate / 5 h / 50 °C
With
copper(l) iodide; palladium diacetate; potassium carbonate; diisopropylamine; triphenylphosphine; potassium iodide;
In
ethyl acetate; N,N-dimethyl-formamide;
3: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.02.118
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 15 h / 100 °C
2: palladium diacetate; triphenylphosphine; copper(l) iodide; diisopropylamine / ethyl acetate / 5 h / 50 °C
With
copper(l) iodide; palladium diacetate; potassium carbonate; diisopropylamine; triphenylphosphine; potassium iodide;
In
ethyl acetate; N,N-dimethyl-formamide;
2: |Sonogashira Cross-Coupling;
DOI:10.1016/j.bmcl.2013.02.118