2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

Base Information

Chemical Name:2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester
CAS No.:17275-89-7
Molecular Formula:C₁₃H₁₅BrO₅
Molecular Weight:331.163
Hs Code.:

Synonyms:

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Chemical Property of 2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

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Technology Process of 2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

There total 10 articles about 2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17275-82-0
ethyl 3,5-dimethoxybenzoate

: 17275-89-7
2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

Guidance literature:: Multi-step reaction with 9 steps

1: (nitration)

2: H₂ / Raney-Ni / ethanol / 80 - 100 °C / 75 - 90 Torr

3: (i) NaNO₂, aq. HBr, (ii) CuBr, aq. HBr

4: aq. NaOH / ethanol / 120 - 130 °C

5: SOCl₂

6: diethyl ether; benzene

7: Ag₂O, aq. Na₂S₂O₃, Na₂CO₃ / dioxane

8: diethyl ether

9: aq. HClO₄ / acetic acid

With sodium hydroxide; thionyl chloride; perchloric acid; hydrogen; sodium carbonate; sodium thiosulfate; silver(l) oxide; nickel; In 1,4-dioxane; diethyl ether; ethanol; acetic acid; benzene;
DOI:10.1248/cpb.15.1765

Reference yield:

: 17275-83-1
3,5-dimethoxy-2-nitro-benzoic acid ethyl ester

: 17275-89-7
2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

Guidance literature:: Multi-step reaction with 8 steps

1: H₂ / Raney-Ni / ethanol / 80 - 100 °C / 75 - 90 Torr

2: (i) NaNO₂, aq. HBr, (ii) CuBr, aq. HBr

3: aq. NaOH / ethanol / 120 - 130 °C

4: SOCl₂

5: diethyl ether; benzene

6: Ag₂O, aq. Na₂S₂O₃, Na₂CO₃ / dioxane

7: diethyl ether

8: aq. HClO₄ / acetic acid

With sodium hydroxide; thionyl chloride; perchloric acid; hydrogen; sodium carbonate; sodium thiosulfate; silver(l) oxide; nickel; In 1,4-dioxane; diethyl ether; ethanol; acetic acid; benzene;
DOI:10.1248/cpb.15.1765

Reference yield:

: 1132-21-4
3,5-dimethoxybenzoic acid

: 17275-89-7
2-Acetyl-6-brom-3,5-dimethoxy-phenylessigsaeure-methylester

Guidance literature:: Multi-step reaction with 10 steps

1: HCl

2: (nitration)

3: H₂ / Raney-Ni / ethanol / 80 - 100 °C / 75 - 90 Torr

4: (i) NaNO₂, aq. HBr, (ii) CuBr, aq. HBr

5: aq. NaOH / ethanol / 120 - 130 °C

6: SOCl₂

7: diethyl ether; benzene

8: Ag₂O, aq. Na₂S₂O₃, Na₂CO₃ / dioxane

9: diethyl ether

10: aq. HClO₄ / acetic acid

With hydrogenchloride; sodium hydroxide; thionyl chloride; perchloric acid; hydrogen; sodium carbonate; sodium thiosulfate; silver(l) oxide; nickel; In 1,4-dioxane; diethyl ether; ethanol; acetic acid; benzene;
DOI:10.1248/cpb.15.1765