AKOS BB-9147

Base Information

• Chemical Name: AKOS BB-9147
• CAS No.: 408328-22-3
• Molecular Formula: C₇H₃BrN₂O₂S
• Molecular Weight: 259.083
• Mol file: 408328-22-3.mol

Synonyms:

Chemical Property of AKOS BB-9147

Chemical Property:

• Boiling Point: 316.2±32.0 °C(Predicted)
• Density: 1.85±0.1 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

4-Bromo-3-nitrophenyl thiocyanate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of AKOS BB-9147

There total 5 articles about AKOS BB-9147 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-nitro-4-thiocyanoaniline (54029-45-7) → 4-bromo-3-nitro-phenyl thiocyanate (408328-22-3)

Guidance literature:

With hydrogen bromide; bromine; anschliessend Behandeln mit wss. Natriumnitrit-Loesung;

DOI:10.1021/jo01139a015

Reference yield:

2-nitro-aniline (88-74-4) → 4-bromo-3-nitro-phenyl thiocyanate (408328-22-3)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous acetic acid; bromine

2: aqueous hydrobromic acid; bromine / anschliessend Behandeln mit wss. Natriumnitrit-Loesung

With hydrogen bromide; bromine; acetic acid;

DOI:10.1021/jo01139a015

Reference yield:

→ 4-bromo-3-nitro-phenyl thiocyanate (408328-22-3)

Guidance literature:

With bromine; copper(I) bromide;

upstream raw materials:

2-nitro-4-thiocyanoaniline

4-bromo-3-nitroaniline

potassium thioacyanate

2-nitro-aniline