Technology Process of C29H34N12O8
There total 10 articles about C29H34N12O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-iodo-succinimide; trifluorormethanesulfonic acid;
In
diethyl ether; dichloromethane;
at 20 ℃;
for 1h;
optical yield given as %de;
stereoselective reaction;
Inert atmosphere;
DOI:10.1021/jo200951p
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dmap; triflic azide / dichloromethane / 45 h / 20 °C / Inert atmosphere
2: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere
3: water; acetic acid / 1.5 h / 70 °C / Inert atmosphere
4: pyridine / N,N-dimethyl-formamide / -15 °C / Inert atmosphere
5: sodium azide / N,N-dimethyl-formamide / 10.5 h / 80 °C / Inert atmosphere
6: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere
With
pyridine; dmap; N-iodo-succinimide; sodium azide; trifluorormethanesulfonic acid; triflic azide; water; sodium hydride; acetic acid;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200951p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium azide / N,N-dimethyl-formamide / 10.5 h / 80 °C / Inert atmosphere
2: N-iodo-succinimide; trifluorormethanesulfonic acid / diethyl ether; dichloromethane / 1 h / 20 °C / Inert atmosphere
With
N-iodo-succinimide; sodium azide; trifluorormethanesulfonic acid;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo200951p