3'-benzyl-S-adenosylmethionine iodide

Base Information

• Chemical Name: 3'-benzyl-S-adenosylmethionine iodide
• CAS No.: 1341220-55-0
• Molecular Formula: C₂₂H₂₉N₆O₅S*I
• Molecular Weight: 616.48

Synonyms:

Chemical Property of 3'-benzyl-S-adenosylmethionine iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-benzyl-S-adenosylmethionine iodide

There total 9 articles about 3'-benzyl-S-adenosylmethionine iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.4%

(S)-2-amino-4-((((2S,3S,4R,5R)-5-(6-amino-9H-purin-9-yl)-3-(benzyloxy)-4-hydroxytetrahydrofuran-2-yl)methyl)thio)butanoic acid (1341220-51-6) + methyl iodide (74-88-4) → 3'-benzyl-S-adenosylmethionine iodide (1341220-55-0)

Guidance literature:

With formic acid; at 25 ℃; for 96h; Darkness;

DOI:10.1021/jm201000j

Reference yield:

phenyldiazomethane (908094-04-2) → 3'-benzyl-S-adenosylmethionine iodide (1341220-55-0)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tin(II) chloride dihdyrate / methanol; 1,2-dimethoxyethane / 25 °C / Inert atmosphere

1.2: 5 h / 25 °C

2.1: sodium hydroxide / water / 1.5 h / 100 °C / Inert atmosphere

2.2: 16 h / 100 °C / Inert atmosphere

3.1: formic acid / 96 h / 25 °C / Darkness

With formic acid; tin(II) chloride dihdyrate; sodium hydroxide; In methanol; 1,2-dimethoxyethane; water;

DOI:10.1021/jm201000j

Reference yield:

N-benzyl-p-toluenesulfonamide (1576-37-0) → 3'-benzyl-S-adenosylmethionine iodide (1341220-55-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sodium nitrite / acetic anhydride; acetic acid / 0 - 25 °C

2.1: sodium methylate / methanol; diethyl ether / 0.5 h / Reflux

3.1: tin(II) chloride dihdyrate / methanol; 1,2-dimethoxyethane / 25 °C / Inert atmosphere

3.2: 5 h / 25 °C

4.1: sodium hydroxide / water / 1.5 h / 100 °C / Inert atmosphere

4.2: 16 h / 100 °C / Inert atmosphere

5.1: formic acid / 96 h / 25 °C / Darkness

With formic acid; tin(II) chloride dihdyrate; sodium methylate; sodium hydroxide; sodium nitrite; In methanol; 1,2-dimethoxyethane; diethyl ether; water; acetic anhydride; acetic acid;

DOI:10.1021/jm201000j

upstream raw materials:

(E)-N'-(9-((2R,3R,4S,5S)-5-(chloromethyl)-3,4-dihydroxytetrahydrofuran-2-yl)-9H-purin-6yl)-N,N-dimethylformimidamide

(2R,3R,4S,5S)-2-(6-amino-9H-purin-9-yl)-4-(benzyloxy)-5-(chloromethyl)tetrahydrofuran-3-ol

(S)-2-amino-4-((((2S,3S,4R,5R)-5-(6-amino-9H-purin-9-yl)-3-(benzyloxy)-4-hydroxytetrahydrofuran-2-yl)methyl)thio)butanoic acid

methyl iodide

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1341220-55-0 3'-benzyl-S-adenosylmethionine iodide

Send

Send

Metric Ton KG G Pound L ML

Send

Send