TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3

Base Information

• Chemical Name: TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3
• CAS No.: 344780-13-8
• Molecular Formula: C₂₃H₂₅Cl₃NPTi
• Molecular Weight: 500.671
• Mol file: 344780-13-8.mol

Synonyms:

Chemical Property of TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3

Chemical Property:

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Useful:

Technology Process of TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3

There total 1 articles about TiCl₃NP(C₆H₅)2CH₂C₆H₄C(CH₃)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(CH3)3SiNP(C6H5)2CH2C6H4C(CH3)3 (344780-11-6) + titanium tetrachloride (7550-45-0) → TiCl3NP(C6H5)2CH2C6H4C(CH3)3 (344780-13-8) + TiCl3NSi(CH3)3P(C6H5)2CHC6H4C(CH3)3 (344780-12-7)

Guidance literature:

In toluene; byproducts: (CH3)3SiCl; (N2); addn. dropwise a soln. of TiCl4 in toluene to a soln. of ligand intoluene at -78°C over a period of 10 min, warming to room temp., stirring for 32 h; concn., addn. of light petroleum ether, drying in vac.; elem. anal.;

DOI:10.1039/b009082o

upstream raw materials:

(CH₃)3SiNP(C₆H₅)2CH₂C₆H₄C(CH₃)3

titanium tetrachloride