(CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

Base Information

Chemical Name:(CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2
CAS No.:416874-80-1
Molecular Formula:C₃₈H₅₀Cl₂N₄Pd₂
Molecular Weight:846.588
Hs Code.:

(CH<sub>3</sub>C<sub>4</sub>H<sub>2</sub>NCCH<sub>3</sub>NC<sub>6</sub>H<sub>3</sub>(C<sub>3</sub>H<sub>7</sub>)2PdCl)2

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Chemical Property of (CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

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Technology Process of (CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

There total 1 articles about (CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: sodium tetrachloropalladate(II)

: 375825-45-9
1-(1-(5-methylpyrrole-2-yl)ethylidene)amino-2,6-diisopropylbenzene

: 416874-80-1,417708-74-8
(CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

Guidance literature:: With sodium acetate; In methanol; pyrrol-compound and sodium acetate in methanol were added to the cooled to -40°C soln. of Pd-compound in methanol, the mixt. was warmed and stirred at room temp. for 12 h; filtered, washed with methanol, air-dried, recrystd. from CH2Cl2-methanol; elem. anal.;
DOI:10.1021/om010968j

Reference yield: 85.0%

: 416874-80-1,417708-74-8
(CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

: 1207973-75-8
lithium tert-butyl acetate

: 416874-83-4
CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2Pd(C₄H₈O)CH₂CO₂C₄H₉

Guidance literature:: In tetrahydrofuran; a soln. of complex in THF was added to a soln. of Li-compound in THF at -78°C, stirred at -78°c for 2 h, allowed to warm to room temp. during 12 h; the solvent was removed in vac., extd. with ether, filtered, evapd., theoil was solidified upon addn. of pentane;
DOI:10.1021/om010968j

Reference yield: 76.0%

: 416874-80-1,417708-74-8
(CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2PdCl)2

: 1207973-75-8
lithium tert-butyl acetate

: 603-35-0
triphenylphosphine

: 416874-88-9
CH₃C₄H₂NCCH₃NC₆H₃(C₃H₇)2Pd(P(C₆H₅)3)CH₂CO₂C₄H₉

Guidance literature:: In tetrahydrofuran; the mixt. in THF was stirred at -78°C for 2 h then at room temp. for 12 h; the solvent was removed in vac., extd. with hexane, filtered, evapd., crystd. from hexane at -20°C; elem. anal.;
DOI:10.1021/om010968j