(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

Base Information

Chemical Name:(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2
CAS No.:944160-02-5
Molecular Formula:C₃₃H₅₃BFeN₂
Molecular Weight:544.455
Hs Code.:

Synonyms:

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Chemical Property of (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

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Technology Process of (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

There total 2 articles about (2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 97-94-9
triethyl borane

: 854669-50-4
[(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)]2

: 506406-67-3
NacNacFe-Et

: 944160-02-5
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

Guidance literature:: In hexane; toluene; under N2; Fe complex dissolved in toluene; BEt3 in hexane added; heated at 70°C for 14 h; volatiles removed under vac.; extd. with pentane; filtered; concd.; crystd. from pentane at -35°C (Fe-B complex); elem. anal.;
DOI:10.1021/om7003805

Reference yield: 72.0%

: (2-((2,6-diisopropylphenyl)amino)-4-((2,6-diisopropylphenyl)imino)-pent-2-ene) lithium salt

: iron(II) chloride*1.5THF

: potassium triethylborohydride

: 944160-02-5
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

Guidance literature:: In toluene; under N2; mixt. of Li salt of ligand and Fe complex in toluene stirred at 80°C for 22 h; solvent removed in vac.; soln. of KHBEt3 in toluene added; heated at 80°C for 4 h; volatiles removed under vac.; extd. with pentane; filtered; concd.; crystd. from pentane at -35°C; elem. anal.;
DOI:10.1021/om7003805

Reference yield: 90.0%

: 944160-02-5
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(μ-H)2BEt2

: 302-01-2,78206-91-4,119775-10-9,75013-58-0
hydrazine

: 944160-06-9
(2,4-bis(2,6-diisopropylphenylimino)pent-3-yl)Fe(hydrazine)(μ-H)2BEt2

Guidance literature:: In diethyl ether; under N2; Fe complex dissolved in Et2O; hydrazine added; shaken; concd.; crystd. at -35°C; elem. anal.;
DOI:10.1021/om7003805