MesSn(OCH₂CH₂NMe₂)2Cl

Base Information

• Chemical Name: MesSn(OCH₂CH₂NMe₂)2Cl
• CAS No.: 1104076-75-6
• Molecular Formula: C₁₇H₃₁ClN₂O₂Sn
• Molecular Weight: 449.608
• Mol file: 1104076-75-6.mol

Synonyms:

Chemical Property of MesSn(OCH₂CH₂NMe₂)2Cl

Chemical Property:

Purity/Quality:

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Technology Process of MesSn(OCH₂CH₂NMe₂)2Cl

There total 1 articles about MesSn(OCH₂CH₂NMe₂)2Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

trichloro(mesityl)stannane (108343-64-2) + methyltin(IV) trichloride (993-16-8) → MesSn(OCH2CH2NMe2)2Cl (1104076-75-6)

Guidance literature:

In tetrahydrofuran; byproducts: Et3SnCl; under Ar; a soln. of MesSnCl3 (6.10 mmol) in THF was added dropwise to astirred soln. of Et3Sn-contg. compd. (13.43 mmol) in THF; the mixt. was stirred for 2 h and stored overnight; the solvent was removed in vac. to ca. 1/6 of the initial vol.; hexane was added; the ppt. was filtered, washed with hexane and dried in vac.; elem. anal.;

DOI:10.1016/j.jorganchem.2008.09.043

upstream raw materials:

trichloro(mesityl)stannane

methyltin(IV) trichloride