Technology Process of Stannane, trichloro(2,4,6-trimethylphenyl)-
There total 4 articles about Stannane, trichloro(2,4,6-trimethylphenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
toluene;
N2-atmosphere; slow addn. of slight excess SnCl4 to Cu-compd. at -30°C, slow warming to room temp., stirring for 12 h, heating to 50°C for 1 h; filtration, removal of volatiles (vac.), recrystn. (hexanes, -55°C);
DOI:10.1021/om9901224
- Guidance literature:
-
Multi-step reaction with 2 steps
1: acetonitrile
In
acetonitrile;
- Guidance literature:
-
In
toluene;
formation of suspension of mesityllithium from bromomesitylene and n-butyllithium in n-hexane and react. of suspension with tin tetrachloride in toluene at about 10°C; stirring of react. mixture 8h at room temp. and refluxing for 24h;; after sepn. of salts, fractionating distn. (113°C/0.03mbar);;
DOI:10.1016/0022-328X(91)80134-6
![[mesitylcopper]5 * toluene](/Databaselist/images/loading.webp)
