(S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester

Base Information

• Chemical Name: (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester
• CAS No.: 61570-06-7
• Molecular Formula: C₂₆H₂₇NO₆
• Molecular Weight: 449.503

Synonyms:

Chemical Property of (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester

There total 4 articles about (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-phenyl-(2,2,2-trichloro-ethoxycarbonyloxy)-acetic acid (3aR)-2-methoxy-(3arC4,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester (61586-85-4) → (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC4,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester (61570-06-7)

Guidance literature:

With acetic acid; zinc; Ambient temperature;

DOI:10.1021/jm00213a002

Reference yield:

(S)-benzyl 2-hydroxy-2-phenylacetate (62173-99-3) → (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC4,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester (61570-06-7)

Guidance literature:

Multi-step reaction with 3 steps

2: (i) H₂, Pd-C, THF, (ii) oxalyl dichloride, (iii) /BRN= 628324/, Py, CH₂Cl₂

3: Zn, AcOH / Ambient temperature

With acetic acid; zinc;

DOI:10.1021/jm00213a002

Reference yield:

(S)-phenyl-(2,2,2-trichloro-ethoxycarbonyloxy)-acetic acid benzyl ester (61566-80-1) → (S)-hydroxy-phenyl-acetic acid (3aR)-2-methoxy-(3arC4,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester (61570-06-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (i) H₂, Pd-C, THF, (ii) oxalyl dichloride, (iii) /BRN= 628324/, Py, CH₂Cl₂

2: Zn, AcOH / Ambient temperature

With acetic acid; zinc;

DOI:10.1021/jm00213a002

upstream raw materials:

(S)-phenyl-(2,2,2-trichloro-ethoxycarbonyloxy)-acetic acid (3aR)-2-methoxy-(3arC⁴,14bc)-1,5,6,8,9,14b-hexahydro-4H-cyclopenta[b][1,3]dioxolo[4',5':4,5]benzo[1,2-d]pyrrolo[1,2-a]azepin-1t-yl ester

(S)-benzyl 2-hydroxy-2-phenylacetate

(S)-phenyl-(2,2,2-trichloro-ethoxycarbonyloxy)-acetic acid benzyl ester

cephalotaxine

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