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Technology Process of (C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]

(C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]

Base Information Edit
  • Chemical Name:(C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]
  • CAS No.:1188001-94-6
  • Molecular Formula:C16H32LiO4*C46H58Si2Y
  • Molecular Weight:1051.41
  • Hs Code.:
  • Mol file:1188001-94-6.mol
(C<sub>9</sub>H<sub>6</sub>Si(CH<sub>3</sub>)2(CH<sub>2</sub>)2Si(CH<sub>3</sub>)2C<sub>9</sub>H<sub>6</sub>)Y(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2<sup>(1-)</sup>*Li(OC<sub>4</sub>H<sub>8</sub>)4<sup>(1+)</sup>=[((C<sub>9</sub>H<sub>6</sub>Si(CH<sub>3</sub>)2CH<sub>2</sub>)2)Y(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>4</sub>H<sub>9</sub>)2][Li(OC<sub>4</sub>H<sub>8</sub>)4]

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Suppliers and Price of (C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]
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Chemical Property of (C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4] Edit
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Technology Process of (C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]

There total 1 articles about (C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

1,2-bis(chlordimethylsilyl)ethane
130713-90-5

1,2-bis(chlordimethylsilyl)ethane

Li(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>4</sub>H<sub>9</sub>)
46061-17-0

Li(CH2C6H4C4H9)

yttrium(III) chloride
10361-92-9,61894-01-7

yttrium(III) chloride

(C<sub>9</sub>H<sub>6</sub>Si(CH<sub>3</sub>)2(CH<sub>2</sub>)2Si(CH<sub>3</sub>)2C<sub>9</sub>H<sub>6</sub>)Y(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C(CH<sub>3</sub>)3)2<sup>(1-)</sup>*Li(OC<sub>4</sub>H<sub>8</sub>)4<sup>(1+)</sup>=[((C<sub>9</sub>H<sub>6</sub>Si(CH<sub>3</sub>)2CH<sub>2</sub>)2)Y(CH<sub>2</sub>C<sub>6</sub>H<sub>4</sub>C<sub>4</sub>H<sub>9</sub>)2][Li(OC<sub>4</sub>H<sub>8</sub>)4]
1188001-94-6

(C9H6Si(CH3)2(CH2)2Si(CH3)2C9H6)Y(CH2C6H4C(CH3)3)2(1-)*Li(OC4H8)4(1+)=[((C9H6Si(CH3)2CH2)2)Y(CH2C6H4C4H9)2][Li(OC4H8)4]

Guidance literature:
In tetrahydrofuran; byproducts: LiCl; (Ar); std. Schlenk technique; soln. of Li salt in THF was added dropwiseto suspn. of YCl3 in THF at room temp.; stirred at room temp. for 3 h; soln. of indenyl ligand in THF was added slowly; stirred at room temp. f or 2 h; evapd. (vac.); extd. (toluene); centrifuged; evapd. (vac.); dissolved intoluene/THF (2/1); cooled to -30°C for several d; elem. anal.;
DOI:10.1016/j.jorganchem.2009.04.033
upstream raw materials:

1,2-bis(chlordimethylsilyl)ethane

Li(CH2C6H4C4H9)

yttrium(III) chloride

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