26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

Base Information

• Chemical Name: 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid
• CAS No.: 124175-39-9
• Molecular Formula: C₄₃H₆₀O₈
• Molecular Weight: 704.945

Synonyms:

Chemical Property of 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

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Technology Process of 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid

There total 5 articles about 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.010,15]octacosa-1(27),10(15),11,13,24(28),25-hexaene-28-carboxylic acid methyl ester (119271-50-0) → 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.010,15]octacosa-1(27),10(15),11,13,24(28),25-hexaene-28-carboxylic acid (124175-39-9)

Guidance literature:

With potassium hydroxide; In ethanol; for 18h; Heating;

DOI:10.1021/jm00164a048

Reference yield:

2,4,4-trimethyl-1-pentene (107-39-1) → 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.010,15]octacosa-1(27),10(15),11,13,24(28),25-hexaene-28-carboxylic acid (124175-39-9)

Guidance literature:

Multi-step reaction with 5 steps

1: conc. H₂SO₄ / 2 h / 130 °C

2: potassium carbonate / dimethylformamide / 20 h / 140 °C

3: 1 N HCl / methanol / Ambient temperature

4: 37 percent / 50percent sodium hydride / tetrahydrofuran / Ambient temperature

5: 1.4 M KOH / ethanol / 18 h / Heating

With hydrogenchloride; potassium hydroxide; sulfuric acid; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00164a048

Reference yield:

3-(2-phenethyl)catechol (350686-32-7) → 26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.010,15]octacosa-1(27),10(15),11,13,24(28),25-hexaene-28-carboxylic acid (124175-39-9)

Guidance literature:

Multi-step reaction with 5 steps

1: conc. H₂SO₄ / 2 h / 130 °C

2: potassium carbonate / dimethylformamide / 20 h / 140 °C

3: 1 N HCl / methanol / Ambient temperature

4: 37 percent / 50percent sodium hydride / tetrahydrofuran / Ambient temperature

5: 1.4 M KOH / ethanol / 18 h / Heating

With hydrogenchloride; potassium hydroxide; sulfuric acid; sodium hydride; potassium carbonate; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;

DOI:10.1021/jm00164a048

upstream raw materials:

26-tert-Butyl-11-phenethyl-13-(1,1,3,3-tetramethyl-butyl)-3,6,9,16,19,22-hexaoxa-tricyclo[22.3.1.0^10,15]octacosa-1⁽²⁷⁾,10⁽¹⁵⁾,11,13,24⁽²⁸⁾,25-hexaene-28-carboxylic acid methyl ester

2,4,4-trimethyl-1-pentene

3-(2-phenethyl)catechol

C₄₀H₆₂O₈

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