(+/-)-sclerone acetonide

Base Information

Chemical Name:(+/-)-sclerone acetonide
CAS No.:19741-76-5
Molecular Formula:C₁₃H₁₄O₃
Molecular Weight:218.252
Hs Code.:

Synonyms:

Suppliers and Price of (+/-)-sclerone acetonide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-sclerone acetonide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-sclerone acetonide

There total 1 articles about (+/-)-sclerone acetonide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6312-53-4
juglone

: 77-76-9
2,2-dimethoxy-propane

: 51114-98-8,54712-38-8,62332-73-4,137494-04-3
isosclerone

: 19741-76-5
(+/-)-sclerone acetonide

Guidance literature:: With lithium aluminium tetrahydride; camphor-10-sulfonic acid; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, ether; 2.) r.t, 30-40 min;
DOI:10.1248/cpb.34.4540

Reference yield:

: 19741-76-5
(+/-)-sclerone acetonide

: 88899-03-0,110901-26-3,110901-27-4
2α,4α,5-trihydroxy-1-tetralone

Guidance literature:: Multi-step reaction with 2 steps

1: 12 mg / 1.) butyl lithium, diisopropylamine; 2.) MoO₅*HMPA / 1.) hexane, THF, -70 deg C, 20 min; 2:) THF, -25 deg C, 30 min

2: 3 mg / 5percent HCl / tetrahydrofuran / 1 h / Ambient temperature

With hydrogenchloride; n-butyllithium; molybdenum peroxide hexamethylphosphorylamide; diisopropylamine; In tetrahydrofuran;
DOI:10.1248/cpb.34.4540