Mo(IV)(O)(ttp)

Base Information

Chemical Name:Mo(IV)(O)(ttp)
CAS No.:64024-42-6
Molecular Formula:C₄₈H₃₆MoN₄O
Molecular Weight:780.78
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mo(IV)(O)(ttp)

Chemical Property:

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Technology Process of Mo(IV)(O)(ttp)

There total 11 articles about Mo(IV)(O)(ttp) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

: 64024-42-6
Mo(IV)(O)(ttp)

: 91156-35-3
cis-(meso-tetra-p-tolylporphyrinato)Mo(CO)2

Guidance literature:: With CO; zinc amalgam; In benzene; CO was bubbled in a benzene soln. of the Mo complex in presence of Zn amalgam, stirred overnight at room temp. under 1.5 atm CO; filtered, evapd. to dryness, crystd. from mesitylene-heptane in darkness under CO;

Reference yield: 19.0%

: lithium sulfide

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

: 165070-95-1
sulfido(5,10,15,20-tetra-p-tolylporphyrinato)molybdenum(IV)

: 64024-42-6
Mo(IV)(O)(ttp)

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; inert atmosphere; stirring (40 - 50°C, 10 h); cooling to room temp., evapn. to dryness, dissolving in toluene, chromy. (neutral alumina/toluene), collection of first band, solvent removal (vac.), dissolving in toluene, layering (hexanes), cooling (-20°C,36 h);

Reference yield: 17.0%

: sodium selenide

: 64024-40-4
(meso-tetra-p-tolylporphyrinato)MoCl₂

: 64024-42-6
Mo(IV)(O)(ttp)

: 165070-96-2
selenido(5,10,15,20-tetra-p-tolylporphyrinato)molybdenum(IV)

Guidance literature:: In tetrahydrofuran; byproducts: NaCl; inert atmosphere; stirring (40 - 50°C, 24 h); cooling (room temp.), evapn. to dryness, dissoving (toluene), chromy. (neutral alumina/toluene), collection orange/red band, solvent removal (vac.), dissloving in toluene, layering (hexanes), drying (vac.); elem. anal.;