2,2-dinitro-tetra-ortho-azobenzene

Base Information

Chemical Name:2,2-dinitro-tetra-ortho-azobenzene
CAS No.:1346157-78-5
Molecular Formula:C₃₀H₂₀N₁₀O₄
Molecular Weight:584.553
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-dinitro-tetra-ortho-azobenzene

Chemical Property:

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Technology Process of 2,2-dinitro-tetra-ortho-azobenzene

There total 6 articles about 2,2-dinitro-tetra-ortho-azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 98081-72-2
2,2'-((E,E)-1,2-phenylenbisazo)dianiline

: 612-29-3
o-nitronitrosobenzene

: 1346157-78-5
2,2-dinitro-tetra-ortho-azobenzene

Guidance literature:: In acetic acid; toluene; at 60 ℃; for 96h; Inert atmosphere;
DOI:10.1021/jo201996w

Reference yield:

: 21354-01-8
N-(2-nitrosophenyl)acetamide

: 1346157-78-5
2,2-dinitro-tetra-ortho-azobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: acetic acid; toluene / 21 h / 60 °C / Inert atmosphere

2: acetic acid / 21 h / 60 °C / Inert atmosphere

3: potassium hydroxide / ethanol; water / 1.5 h / 90 °C

4: acetic acid; toluene / 96 h / 60 °C / Inert atmosphere

With potassium hydroxide; In ethanol; water; acetic acid; toluene; 1: Mills reaction / 2: Mills reaction / 4: Mills reaction;
DOI:10.1021/jo201996w

Reference yield:

: 95-54-5
1,2-diamino-benzene

: 1346157-78-5
2,2-dinitro-tetra-ortho-azobenzene

Guidance literature:: Multi-step reaction with 6 steps

1: ethyl acetate / 0.33 h / 5 °C / Cooling with ice

2: oxone / dichloromethane; water / 1 h / 20 °C

3: acetic acid; toluene / 21 h / 60 °C / Inert atmosphere

4: acetic acid / 21 h / 60 °C / Inert atmosphere

5: potassium hydroxide / ethanol; water / 1.5 h / 90 °C

6: acetic acid; toluene / 96 h / 60 °C / Inert atmosphere

With oxone; potassium hydroxide; In ethanol; dichloromethane; water; acetic acid; ethyl acetate; toluene; 3: Mills reaction / 4: Mills reaction / 6: Mills reaction;
DOI:10.1021/jo201996w