Technology Process of C21H31N3O8
There total 7 articles about C21H31N3O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sodium hydrogencarbonate / 1,4-dioxane; water
2: tetrabutyl ammonium fluoride / tetrahydrofuran
3: sodium hydride / N,N-dimethyl-formamide / 0 - 20 °C
4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / pH 7
5: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / Molecular sieve
6: methoxybenzene; trifluoroacetic acid / dichloromethane
With
tetrabutyl ammonium fluoride; sodium hydride; sodium hydrogencarbonate; methoxybenzene; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/co200161z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / Molecular sieve
2: methoxybenzene; trifluoroacetic acid / dichloromethane
With
tetrabutyl ammonium fluoride; methoxybenzene; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/co200161z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran; N,N-dimethyl-formamide / Molecular sieve
2: methoxybenzene; trifluoroacetic acid / dichloromethane
With
tetrabutyl ammonium fluoride; methoxybenzene; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/co200161z
