Technology Process of C31H31N5O6S
There total 8 articles about C31H31N5O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 0 - 20 ℃;
for 3h;
DOI:10.1021/jm201591k
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate / methanol / 20 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
With
sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm201591k
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / -40 - 20 °C
2: manganese(IV) oxide / dichloromethane / 20 °C
3: sodium acetate / methanol / 1 h / 20 °C
4: sodium tetrahydroborate / methanol / 20 °C
5: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / 0 - 20 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 0 - 20 °C
With
manganese(IV) oxide; sodium tetrahydroborate; lithium aluminium tetrahydride; sodium acetate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm201591k