C₆H₅CH₂(NC₄H₇)CON(C₆H₄)C(CH₃)NCH₂COOCuOH₂*0.5H₂O

Base Information

• Chemical Name: C₆H₅CH₂(NC₄H₇)CON(C₆H₄)C(CH₃)NCH₂COOCuOH₂*0.5H₂O
• CAS No.: 83528-07-8
• Molecular Formula: C₂₂H₂₅CuN₃O₄*0H₂O
• Molecular Weight: 468.012
• Mol file: 83528-07-8.mol

Synonyms:

Chemical Property of C₆H₅CH₂(NC₄H₇)CON(C₆H₄)C(CH₃)NCH₂COOCuOH₂*0.5H₂O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆H₅CH₂(NC₄H₇)CON(C₆H₄)C(CH₃)NCH₂COOCuOH₂*0.5H₂O

There total 1 articles about C₆H₅CH₂(NC₄H₇)CON(C₆H₄)C(CH₃)NCH₂COOCuOH₂*0.5H₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper(ll) sulfate pentahydrate + (S)-o-<(N-benzylprolyl)amino>acetophenone (82704-15-2) + glycine (56-40-6,18875-39-3,25718-94-9) → C6H5CH2(NC4H7)CON(C6H4)C(CH3)NCH2COOCuOH2*0.5H2O (83528-07-8)

Guidance literature:

With NaOCH₃; In methanol; water; under Ar, glycine in CH3ONa/methanol, (S)-2-N-(N'-benzylprolyl)aminoacetophenone and molecular sieve (3 Angstroem) stirred at room temp. for 15min, filtered, CuSO4*5H2O in water added, stirred for 45 min, 1 N CH3ONa in H2O/CHCl3 added; extd. (CHCl3), purified (silica gel, C2H5OH); elem. anal.;

DOI:10.1021/ja00345a057

upstream raw materials:

(S)-o-<(N-benzylprolyl)amino>acetophenone

glycine