Cyclohexanol, 2-[(phenylmethoxy)methyl]-, cis-

Base Information

Chemical Name:Cyclohexanol, 2-[(phenylmethoxy)methyl]-, cis-
CAS No.:138630-56-5
Molecular Formula:C14H20O2
Molecular Weight:220.312
Hs Code.:

Synonyms:

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Chemical Property of Cyclohexanol, 2-[(phenylmethoxy)methyl]-, cis-

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Technology Process of Cyclohexanol, 2-[(phenylmethoxy)methyl]-, cis-

There total 7 articles about Cyclohexanol, 2-[(phenylmethoxy)methyl]-, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 25662-37-7
methyl cyclohex-2-en-1-carboxylate

: 138630-56-5
cis-2-<(benzyloxy)methyl>cyclohexanol

Guidance literature:: Multi-step reaction with 5 steps

1: 5.6 g / LiAlH₄ / diethyl ether / 3 h / Heating

2: NaH / tetrahydrofuran

3: 3.6 g / t-BuOOH, TiCl₄ / CH₂Cl₂; 2,2,4-trimethyl-pentane / -78 °C

4: 2.1 g / t-BuOK / benzene

5: 0.16 g / LiAlH₄ / pentane / 2 h

With tert.-butylhydroperoxide; lithium aluminium tetrahydride; potassium tert-butylate; titanium tetrachloride; sodium hydride; In tetrahydrofuran; 2,2,4-trimethylpentane; diethyl ether; dichloromethane; pentane; benzene;
DOI:10.1021/jo00032a022

Reference yield:

: 138630-47-4
c-3-<(benzyloxy)methyl>-r-1,2-epoxycyclohexane

: 138630-56-5
cis-2-<(benzyloxy)methyl>cyclohexanol

Guidance literature:: With lithium aluminium tetrahydride; In pentane; for 2h;
DOI:10.1021/jo00032a022

Reference yield:

: 103668-33-3,3309-97-5
3-hydroxymethylcyclohexene

: 138630-56-5
cis-2-<(benzyloxy)methyl>cyclohexanol

Guidance literature:: Multi-step reaction with 4 steps

1: NaH / tetrahydrofuran

2: 3.6 g / t-BuOOH, TiCl₄ / CH₂Cl₂; 2,2,4-trimethyl-pentane / -78 °C

3: 2.1 g / t-BuOK / benzene

4: 0.16 g / LiAlH₄ / pentane / 2 h

With tert.-butylhydroperoxide; lithium aluminium tetrahydride; potassium tert-butylate; titanium tetrachloride; sodium hydride; In tetrahydrofuran; 2,2,4-trimethylpentane; dichloromethane; pentane; benzene;
DOI:10.1021/jo00032a022