Technology Process of C27H24
There total 1 articles about C27H24 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
bis(4-methylphenyl)phenylmethanol; aniline hydrochloride;
In
acetic acid;
for 3h;
Reflux;
With
sulfuric acid; isopentyl nitrite;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
Cooling with ice;
With
phosphinic acid;
In
N,N-dimethyl-formamide;
DOI:10.1002/chem.201302951
- Guidance literature:
-
With
N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile);
In
tetrachloromethane;
for 12h;
Reflux;
DOI:10.1002/chem.201302951
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 12 h / Reflux
2: cesiumhydroxide monohydrate / methanol; N,N-dimethyl-formamide / 18 h / 20 °C
With
N-Bromosuccinimide; cesiumhydroxide monohydrate; 2,2'-azobis(isobutyronitrile);
In
methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201302951