V(Mecalix)NPh

Base Information

Chemical Name:V(Mecalix)NPh
CAS No.:913724-97-7
Molecular Formula:C₅₁H₆₀NO₄V
Molecular Weight:801.983
Hs Code.:

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Suppliers and Price of V(Mecalix)NPh

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of V(Mecalix)NPh

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Technology Process of V(Mecalix)NPh

There total 2 articles about V(Mecalix)NPh which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 45951-52-8
(phenylimido)vanadium(V) trichloride

: 124690-16-0,126186-30-9
5,11,17,23-tetra-tert-butyl-25,26,27-trihydroxy-28-methyloxycalix[4]arene

: 913724-97-7
V(Mecalix)NPh

Guidance literature:: With n-butyl lithium; In tetrahydrofuran; hexane; (under Ar, Schlenk); soln. of n-butyllithium in hexane slowly added to soln. of ligand in THF at room temp., stirred at 65°C for 4 h, cooled to room temp., soln. transferred to soln. of V-complex in THF, stirred at 70°C for 4 h; cooled to room temp., volatiles removed in vacuo, ppt. suspended in toluene, filtered, filtrate evapd. to dryness, ppt. suspended in hexane, stirred at 65°C for 1 h, ppt. filtered, dried in vacuo; elem. anal.;
DOI:10.1016/j.ica.2006.06.029