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Technology Process of ((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O

((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O

Base Information
  • Chemical Name:((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O
  • CAS No.:934563-82-3
  • Molecular Formula:C18H25ClFeN3O5*H2O
  • Molecular Weight:472.729
  • Hs Code.:
((CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>12</sub>(CH<sub>2</sub>COO)2)FeCl)*H<sub>2</sub>O

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Chemical Property of ((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O
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Technology Process of ((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O

There total 1 articles about ((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2Li<sup>(1+)</sup>*CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOCH<sub>2</sub>)2<sup>(2-)</sup>=CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N(CH<sub>2</sub>CH<sub>2</sub>NCH<sub>2</sub>COOLiCH<sub>2</sub>)2

2Li(1+)*CH3OC6H4CH2N(CH2CH2NCH2COOCH2)2(2-)=CH3OC6H4CH2N(CH2CH2NCH2COOLiCH2)2

iron(III) chloride
7705-08-0

iron(III) chloride

((CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>12</sub>(CH<sub>2</sub>COO)2)FeCl)*H<sub>2</sub>O
934563-82-3

((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O

Guidance literature:
In methanol; soln. Li salt ligand was added to FeCl3 in MeOH and refluxed for 2 h; soln. was filtered and kept at room temp.; elem. anal.;
DOI:10.1021/ic062001j

Reference yield: 50.0%

sodium azide

sodium azide

((CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>12</sub>(CH<sub>2</sub>COO)2)FeCl)*H<sub>2</sub>O
934563-82-3

((CH3OC6H4CH2N3C6H12(CH2COO)2)FeCl)*H2O

((CH<sub>3</sub>OC<sub>6</sub>H<sub>4</sub>CH<sub>2</sub>N<sub>3</sub>C<sub>6</sub>H<sub>12</sub>(CH<sub>2</sub>COO)2)Fe(N<sub>3</sub>))
934563-83-4

((CH3OC6H4CH2N3C6H12(CH2COO)2)Fe(N3))

Guidance literature:
In methanol; to soln. Fe complex in MeOH NaN3 was added and stirred at room temp. for3 h; ppt. was filtered and recrystd. from MeCN in the dark; elem. anal.;
DOI:10.1021/ic062001j
upstream raw materials:

iron(III) chloride

Downstream raw materials:

((CH3OC6H4CH2N3C6H12(CH2COO)2)Fe(N3))

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