2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide

Base Information

Chemical Name:2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide
CAS No.:6292-80-4
Molecular Formula:C10H12 N4 O S
Molecular Weight:236.2935
Hs Code.:

Synonyms:1,2-Propanedione,1-phenyl-, 2-oxime, thiosemicarbazone (8CI); 1-Phenyl-1,2-propanedione 2-oximethiosemicarbazone; Isonitrosopropiophenone thiosemicarbazone; NSC 9947

Suppliers and Price of 2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide

Chemical Property:

Vapor Pressure:1.94E-05mmHg at 25°C
Boiling Point:362.4°C at 760 mmHg
Flash Point:172.9°C
Density:1.3g/cm³

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide

There total 2 articles about 2-[(1E)-2-nitroso-1-phenylprop-1-en-1-yl]hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 79-19-6
thiosemicarbazide

: 119-51-7
1-phenyl-1,2-propanedione 2-oxime

: 6292-80-4
1-phenyl-1,2-propane dione-2-oxime thiosemicarbazone

Guidance literature:: With hydrogenchloride; In ethanol; water; for 3h; Reflux;
DOI:10.1016/j.apcata.2010.10.003

Reference yield:

: thiosemicarbazine

: 28867-78-9
(Z)-1-phenyl-1,2-propanedione 2-oxime

: 6292-80-4
1-phenyl-1,2-propane dione-2-oxime thiosemicarbazone

Guidance literature:: In water; acetic acid;

Reference yield: 72.0%

: 6292-80-4
1-phenyl-1,2-propane dione-2-oxime thiosemicarbazone

: copper dichloride

: [Cu(1-phenyl-1,2-propanedione-2-oxime thiosemicarbazone)]2Cl₂

Guidance literature:: In ethanol; prepn. by mixing hot ethanolic soln. of metal salt and org. ligand in the molar ratio of 1:1; metal salt soln. added to the boiling soln. of ligand in EtOH and heated under reflux for 3 h; mixt. cooled; left overnight in refrigerator; filtered; washed (hot H2O,cold MeOH);