Technology Process of trans-1-benzoyl-1-(trimethylsilyl)-2-methylcyclopentane
There total 6 articles about trans-1-benzoyl-1-(trimethylsilyl)-2-methylcyclopentane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; chromium(VI) oxide;
In
dichloromethane;
for 0.666667h;
Yield given;
DOI:10.1021/jo00267a032
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) LDA / 1.) -78 deg C, 20 min, 2.) from -30 to -10 deg C, 6 h
2: 82 percent / Dibal-H / CH2Cl2; hexane / 4 h / -10 - 0 °C
3: 720 mg / CrO3, pyridine / CH2Cl2 / 1.5 h / 0 °C
4: 1.60 g / diethyl ether / 0.33 h / -78 °C
5: CrO3, pyridine / CH2Cl2 / 0.67 h
With
pyridine; chromium(VI) oxide; diisobutylaluminium hydride; lithium diisopropyl amide;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo00267a032
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1.) LDA / 1.) -78 deg C, 20 min, 2.) from -30 to -10 deg C, 6 h
2: 82 percent / Dibal-H / CH2Cl2; hexane / 4 h / -10 - 0 °C
3: 720 mg / CrO3, pyridine / CH2Cl2 / 1.5 h / 0 °C
4: 1.60 g / diethyl ether / 0.33 h / -78 °C
5: CrO3, pyridine / CH2Cl2 / 0.67 h
With
pyridine; chromium(VI) oxide; diisobutylaluminium hydride; lithium diisopropyl amide;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1021/jo00267a032
