1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole

Base Information

• Chemical Name: 1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole
• CAS No.: 866128-48-5
• Molecular Formula: C₃₃H₄₂P₂Sn
• Molecular Weight: 619.354
• Mol file: 866128-48-5.mol

Synonyms:

Chemical Property of 1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole

There total 1 articles about 1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[K(THF)P2C3Bu(t)3] + triphenyltin chloride (639-58-7) → 1-triphenylstannyl-2,4,5-tritertiarybutyl-1,3-diphosphole (866128-48-5)

Guidance literature:

In tetrahydrofuran; under Ar atm. using Schlenk techniques; mixt. of K(THF)P2C3(t-Bu)3 and Ph3SnCl in THF stirred for 12 h; suspn. filtered through diatomaceous earth; solvent removed (vac.) from filtrate; recrystd. (cold hexane);

DOI:10.1016/j.jorganchem.2005.05.046

upstream raw materials:

triphenyltin chloride