2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile

Base Information

• Chemical Name: 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile
• CAS No.: 637771-62-1
• Molecular Formula: C₄₀H₁₈F₁₂N₁₂
• Molecular Weight: 894.644

Synonyms:

Chemical Property of 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile

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Technology Process of 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile

There total 1 articles about 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

N4,N5,N4',N5'-Tetrakis-(3-trifluoromethyl-phenyl)-[2,2']biimidazolylidene-4,5,4',5'-tetraamine (189115-08-0) + 2,3-dichloro-5,6-dicyanopyrazine (56413-95-7) → 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile (637771-62-1) + 4,9,4',9'-tetrakis(3-trifluoromethyl-phenyl)-4,9,4',9'-tetrahydro[2,2']bi[1,3,4,5,8,9-hexaazacyclopenta[b]naphthalenylidene]-6,7,6',7'-tetracarbonitrile

Guidance literature:

at 200 ℃; for 0.25h;

DOI:10.3987/com-03-9842

Reference yield: 43.0%

1,1'-Thiocarbonyldiimidazole (6160-65-2) + 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile (637771-62-1) → 2-[5-thioxo-4,6-bis-(3-trifluoromethyl-phenyl)-5,6-dihydro-4H-imidazo[4,5-d]imidazol-2-ylidene]-4,9-bis-(3-trifluoromethyl-phenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaaza-cyclopenta[b]naphthalene-6,7-dicarbonitrile + 2-[5-oxo-4,6-bis-(3-trifluoromethyl-phenyl)-5,6-dihydro-4H-imidazo[4,5-d]imidazol-2-ylidene]-4,9-bis-(3-trifluoromethyl-phenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaaza-cyclopenta[b]naphthalene-6,7-dicarbonitrile

Guidance literature:

at 200 ℃; for 0.25h;

DOI:10.3987/com-03-9842

Reference yield: 29.0%

orthoformic acid triethyl ester (122-51-0) + 2-[4,5-bis-(3-trifluoromethylphenylamino)imidazol-2-ylidene]-4,9-bis-(3-trifluoromethylphenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaazacyclopenta[b]naphthalene-6,7-dicarbonitrile (637771-62-1) → 2-{4,5-bis-[ethyl-(3-trifluoromethyl-phenyl)-amino]-imidazol-2-ylidene}-4,9-bis-(3-trifluoromethyl-phenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaaza-cyclopenta[b]naphthalene-6,7-dicarbonitrile + 2-[5-ethoxy-4,6-bis-(3-trifluoromethyl-phenyl)-5,6-dihydro-4H-imidazo[4,5-d]imidazol-2-ylidene]-4,9-bis-(3-trifluoromethyl-phenyl)-4,9-dihydro-2H-1,3,4,5,8,9-hexaaza-cyclopenta[b]naphthalene-6,7-dicarbonitrile

Guidance literature:

for 12h; Heating;

DOI:10.3987/com-03-9842

upstream raw materials:

N⁴,N⁵,N^4',N^5'-Tetrakis-(3-trifluoromethyl-phenyl)-[2,2']biimidazolylidene-4,5,4',5'-tetraamine

2,3-dichloro-5,6-dicyanopyrazine

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