C₁₃H₁₄F₃NO₂

Base Information

Chemical Name:C₁₃H₁₄F₃NO₂
CAS No.:1361393-71-6
Molecular Formula:C₁₃H₁₄F₃NO₂
Molecular Weight:273.255
Hs Code.:

C<sub>13</sub>H<sub>14</sub>F<sub>3</sub>NO<sub>2</sub>

Synonyms:

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Chemical Property of C₁₃H₁₄F₃NO₂

Chemical Property:

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Technology Process of C₁₃H₁₄F₃NO₂

There total 7 articles about C₁₃H₁₄F₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis-3-hydroxy-2-phenylpiperidine

: 407-25-0
trifluoroacetic anhydride

: 1361393-71-6
C₁₃H₁₄F₃NO₂

Guidance literature:: cis-3-hydroxy-2-phenylpiperidine; trifluoroacetic anhydride; With dmap; triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;

With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 36h; Inert atmosphere;
DOI:10.1039/c2ob06644k

Reference yield:

: dihydro-5-(hydroxy(phenyl)methyl)furan-2(3H)-one

: 1361393-71-6
C₁₃H₁₄F₃NO₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen; potassium carbonate / methanol / 4 h / 20 °C

4.1: borane-THF / 5 h / Inert atmosphere; Reflux

4.2: 0.5 h / 0 - 20 °C / Inert atmosphere

5.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

5.2: 36 h / 20 °C / Inert atmosphere

With dmap; sodium azide; borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06644k

Reference yield:

: C₁₂H₁₄O₅S

: 1361393-71-6
C₁₃H₁₄F₃NO₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium azide / N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen; potassium carbonate / methanol / 4 h / 20 °C

3.1: borane-THF / 5 h / Inert atmosphere; Reflux

3.2: 0.5 h / 0 - 20 °C / Inert atmosphere

4.1: dmap; triethylamine / dichloromethane / 12 h / 20 °C / Inert atmosphere

4.2: 36 h / 20 °C / Inert atmosphere

With dmap; sodium azide; borane-THF; palladium 10% on activated carbon; hydrogen; potassium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2ob06644k