ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl

Base Information

Chemical Name:ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl
CAS No.:1322093-80-0
Molecular Formula:C₃₉H₃₄Au₂Cl₂P₂S₂
Molecular Weight:1093.62
Hs Code.:

ClAu(C<sub>6</sub>H<sub>5</sub>)2PC<sub>4</sub>HS(CH<sub>3</sub>)C<sub>5</sub>H<sub>6</sub>C<sub>4</sub>HS(CH<sub>3</sub>)P(C<sub>6</sub>H<sub>5</sub>)2AuCl

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Chemical Property of ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl

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Technology Process of ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl

There total 1 articles about ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 1190770-22-9
1,2-bis(5-(diphenylphosphino)-2-methylthien-3-yl) cyclopentene

: 1322093-80-0
ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl

Guidance literature:: In dichloromethane; under Ar atm. using Schlenk techniques; soln. of Au complex in CH2Cl2 was added dropwise to soln. of ligand in CH2Cl2 at room temp.; mixt. was stirred for 2 h; solvent removed under vac.; recrystd. (CH2Cl2/n-hexane); elem. anal.;
DOI:10.1021/ic202265u

Reference yield: 48.0%

: 1355078-87-3
5-ethynyl-3-[3,3,4,4,5,5-hexafluoro-2-(2-methyl-5-phenyl-3-thienyl)-1-cyclopenten-1-yl]-2-methylthiophene

: 1322093-80-0
ClAu(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2AuCl

: 1355178-32-3
(C₆H₅)2PC₄HS(CH₃)C₅H₆C₄HS(CH₃)P(C₆H₅)2[C₆H₅C₄HS(CH₃)C₅F₆C₄HS(CH₃)CCAu]2

Guidance literature:: With sodium methoxide; In tetrahydrofuran; methanol; under Ar atm. using Schlenk techniques; Au complex and MeONa were added to dry THF-MeOH (1:1) soln. of ligand with stirring at room temp.; monitored by chromy.; solvent removed under vac.; residue dissolved in CH2Cl2; filtered; layering of n-hexane onto concd. CH2Cl2 soln. gave solid; elem. anal.;
DOI:10.1021/ic202265u