4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

Base Information

Chemical Name:4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine
CAS No.:1620667-06-2
Molecular Formula:C₃₁H₂₀Cl₄N₆S
Molecular Weight:650.418
Hs Code.:

4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

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Chemical Property of 4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

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Technology Process of 4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

There total 5 articles about 4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 504-29-0
2-aminopyridine

: 1620666-98-9
5-(2-chlorobenzylidene)-2-(4-(2-chlorophenyl)-6-(2,4-dichlorophenyl)pyrimidin-2-ylimino)thiazolidin-4-one

: 1620667-06-2
4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

Guidance literature:: In N,N-dimethyl-formamide; for 0.233333h; Microwave irradiation;
DOI:10.1016/j.ejmech.2014.06.033

Reference yield:

: 1354922-08-9
4-(2-chlorophenyl)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

: 1620667-06-2
4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 4 h / Reflux

2: sodium acetate / acetic acid / Microwave irradiation

3: N,N-dimethyl-formamide / 0.23 h / Microwave irradiation

With sodium acetate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.06.033

Reference yield:

: 1620666-96-7
2-(4-(2-chlorophenyl)-6-(2,4-dichlorophenyl)pyrimidin-2-ylimino)thiazolidin-4-one

: 1620667-06-2
4-(2-chlorophenyl)-N-(4-(2-chlorophenyl)-3a,4-dihydro-1H-pyrido[1,2-a]thiazolo[5,4-e]pyrimid in-2(10aH)-ylidene)-6-(2,4-dichlorophenyl)pyrimidin-2-amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / acetic acid / Microwave irradiation

2: N,N-dimethyl-formamide / 0.23 h / Microwave irradiation

With sodium acetate; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2014.06.033