[tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride

Base Information

Chemical Name:[tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride
CAS No.:253325-71-2
Molecular Formula:C₂₂H₂₃AuClNOP
Molecular Weight:580.824
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Chemical Property of [tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride

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Technology Process of [tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride

There total 2 articles about [tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 39929-21-0
(tetrahydrothiophene)gold(I) chloride

: 65754-11-2
N-tert-Butyl-N-(4-diphenylphosphanyl-phenyl)-hydroxylamine

: 253325-71-2
[tert-butyl(p-diphenylphoshinophenyl)aminoxyl]gold chloride

Guidance literature:: With Ag₂O; In dichloromethane; (air); addn. of Ag2O to the ligand in CH2Cl2, stirring (15 min), filtration (Celite), addn. of the soln. to the gold complex, stirring (15 min); solvent removal (vac.), redissoln. (minimum CH2Cl2), running this soln. through a short SiO2 column, removal of solvent (vac.), addn. of Et2O, standing (several h); elem. anal.;