[N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide

Base Information

• Chemical Name: [N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide
• CAS No.: 686290-07-3
• Molecular Formula: C₂₆H₂₂Br₄N₆Ni₂O₆
• Molecular Weight: 951.493
• Mol file: 686290-07-3.mol

Synonyms:

Chemical Property of [N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide

Chemical Property:

Purity/Quality:

Safty Information:

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Useful:

Technology Process of [N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide

There total 1 articles about [N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

dibromo(1,2-dimethoxyethane)nickel(II) + 4-nitro-N-(6-methylpyridin-2-yl)benzamide (37586-00-8) → [N-(6-methyl-2-pyridyl)-4-nitrobenzamide]dinickel(II) di-μ-bromide dibromide (686290-07-3)

Guidance literature:

In tetrahydrofuran; N2; adding THF soln. of ligand to THF soln. of Ni complex, stirring at room temp. for 12 h; filtration, washing the ppt. with THF, vac. drying; elem. anal.;

DOI:10.1016/j.jorganchem.2003.12.022

upstream raw materials:

4-nitro-N-(6-methylpyridin-2-yl)benzamide