6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide

Base Information

• Chemical Name: 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide
• CAS No.: 96671-26-0
• Molecular Formula: C₂₆H₃₇ClN₆O₆S₂
• Molecular Weight: 629.201

Synonyms:

Chemical Property of 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide

Chemical Property:

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Useful:

Technology Process of 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide

There total 5 articles about 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-Chlor-2.4-bis-methylsulfamoyl-anilin (1027-12-9) → 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide (96671-26-0)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) (heating in H₂O), (ii) /BRN= 2009378/

2: (i) ClSO₃H, (ii) liq. NH₃

3: (i) (heating in H₂O), (ii) /BRN= 2705446/

4: aq. HCl, 2,2-dimethoxy-propane / 20 h / 50 °C

With hydrogenchloride; 2,2-dimethoxy-propane;

DOI:10.1021/jo01067a097

Reference yield:

6-chloro-2-methyl-1,1,3-trioxo-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid amide (89813-57-0) → 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide (96671-26-0)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. NaOH

2: (i) (heating in H₂O), (ii) /BRN= 2705446/

3: aq. HCl, 2,2-dimethoxy-propane / 20 h / 50 °C

With hydrogenchloride; sodium hydroxide; 2,2-dimethoxy-propane;

DOI:10.1021/jo01067a097

Reference yield:

6-chloro-2-methyl-1,1,3-trioxo-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-7-sulfonic acid methylamide (135-08-0) → 6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ6-benzo[1,2,4]thiadiazine-3-carboxylic acid 6-[4-(2-methoxy-phenyl)-piperazin-1-yl]-hexylamide (96671-26-0)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) ClSO₃H, (ii) SOCl₂, (iii) liq. NH₃

2: aq. NaOH

3: (i) (heating in H₂O), (ii) /BRN= 2705446/

4: aq. HCl, 2,2-dimethoxy-propane / 20 h / 50 °C

With hydrogenchloride; sodium hydroxide; 2,2-dimethoxy-propane;

DOI:10.1021/jo01067a097

upstream raw materials:

6-(4-(2-methoxyphenyl)piperazin-1-yl)hexan-1-amine

6-Chlor-3.4-dihydro-3-methoxycarbonyl-2-methyl-7-sulfamoyl-2H-1.2.4-benzothiadiazin-1.1-dioxid

5-Chlor-2.4-bis-methylsulfamoyl-anilin

6-chloro-2-methyl-1,1-dioxo-7-sulfamoyl-1,2,3,4-tetrahydro-1λ⁶-benzo[1,2,4]thiadiazine-3-carboxylic acid

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