epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne

Base Information

• Chemical Name: epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne
• CAS No.: 38135-74-9
• Molecular Formula: C₄₂H₂₈O₂
• Molecular Weight: 564.683

Synonyms:

Chemical Property of epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne

Chemical Property:

Purity/Quality:

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Technology Process of epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne

There total 3 articles about epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

N-methylmaleimide (930-88-1) + rubrene endoperoxyde (32287-37-9) → epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

In benzene; at 15 ℃; for 27h; Irradiation;

Reference yield: 2.0%

rubrene endoperoxyde (32287-37-9) → epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

With N-methylmaleimide; In benzene; at 15 ℃; for 27h; Irradiation;

Reference yield:

rubrene endoperoxyde (32287-37-9) → hydroxy-12 triphenyl-6,11,12, oxo-5 dihydro-5,12 naphtacene (98453-01-1) + epoxy-5,12 phenoxy-5 triphenyl-6,11,12 dihydro-5,12 naphtacene (98480-37-6) + 11b-phenoxy-5a,6,11-triphenyl-5a,11b-dihydro-naphto<2,3-3',4'>cyclobuta<1',2',-2,3>benzofuran (98453-02-2) + epoxy-5,13 tetraphenyl-5,7,12,13 dihydro-5,13 benzonaptho<2,3-b>oxepinne (38135-74-9) + N-methyl diepoxy-4a,5:12,12a ethano-1,4 hexahydro-1,4,4a,5,12,12a tetraphenyl-5,6,11,12 naphtacene dicarboximide-13,14 (98453-03-3)

Guidance literature:

In benzene; at 15 ℃; Mechanism; Irradiation; in the presence or absence of N-methylmaleimide;

upstream raw materials:

N-methylmaleimide

rubrene endoperoxyde

Downstream raw materials:

7-o-Benzoylphenyl-6-methoxy-5,7-diphenylbenzofluoren

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