C₂₄H₂₁N₅O₃S

Base Information

Chemical Name:C₂₄H₂₁N₅O₃S
CAS No.:1393736-15-6
Molecular Formula:C₂₄H₂₁N₅O₃S
Molecular Weight:459.528
Hs Code.:

C<sub>24</sub>H<sub>21</sub>N<sub>5</sub>O<sub>3</sub>S

Synonyms:

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Chemical Property of C₂₄H₂₁N₅O₃S

Chemical Property:

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Technology Process of C₂₄H₂₁N₅O₃S

There total 4 articles about C₂₄H₂₁N₅O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1393735-99-3
2-amino-4-chloro-N₂-(4'-cyanophenyl)-5-aminosulfonyl-nitrobenzene

: 1393736-15-6
C₂₄H₂₁N₅O₃S

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 130 °C

2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

2.2: 3 h / 20 °C

3.1: sodium dithionite; ammonium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

With ammonium hydroxide; sodium dithionite; potassium tert-butylate; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm3007678

Reference yield:

: 1393736-01-0
N-(4'-cyanophenyl)-5-(4''-formyl-2'',6''-dimethylphenoxy)-4-aminosulfonyl-2-nitroaniline

: 1393736-15-6
C₂₄H₂₁N₅O₃S

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

1.2: 3 h / 20 °C

2.1: sodium dithionite; ammonium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

With ammonium hydroxide; sodium dithionite; potassium tert-butylate; In tetrahydrofuran; water;
DOI:10.1021/jm3007678

Reference yield:

: 611-06-3
2,4-dichloronitrobenzene

: 1393736-15-6
C₂₄H₂₁N₅O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: chlorosulfonic acid / 0 - 140 °C

2.1: ammonium hydroxide / tetrahydrofuran / 0 °C

3.1: potassium tert-butylate / N,N-dimethyl-formamide / 0 - 20 °C

4.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 130 °C

5.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C

5.2: 3 h / 20 °C

6.1: sodium dithionite; ammonium hydroxide / tetrahydrofuran; water / 2 h / 20 °C

With chlorosulfonic acid; ammonium hydroxide; sodium dithionite; potassium tert-butylate; potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm3007678