(S)-7²-benzoyl-3⁴,7^{6,7_,92_{-tetramethoxy-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester

Base Information

• Chemical Name: (S)-7²-benzoyl-3⁴,7^{6,7_,92_{-tetramethoxy-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester
• CAS No.: 64434-38-4
• Molecular Formula: C₅₄H₅₅N₃O₁₃
• Molecular Weight: 954.043

Synonyms:

Chemical Property of (S)-7²-benzoyl-3⁴,7^{6,7_,92_{-tetramethoxy-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (S)-7²-benzoyl-3⁴,7^{6,7_,92_{-tetramethoxy-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester

There total 1 articles about (S)-7²-benzoyl-3⁴,7^{6,7_,92_{-tetramethoxy-7}1,2,3,4}-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (S)-72-benzoyl-34,76,7,92-tetramethoxy-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester (64434-38-4)

Guidance literature:

Saeure 15b, p-Nitrophenol, Dicyclohexylcarbodiimid;

DOI:10.1248/cpb.25.1636

Reference yield:

(S)-72-benzoyl-34,76,7,92-tetramethoxy-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester (64434-38-4) → 2-benzyl-7,6'-epoxy-6,12'-dimethoxy-2'-methyl-(1'αH)-oxyacanthane (61897-99-2)

Guidance literature:

Multi-step reaction with 5 steps

1: (i) CF₃CO₂H, (ii) Py, DMF

2: POCl₃ / CHCl₃

3: (i) NaBH₄, MeOH, (ii) /BRN= 1209228/, (iii) NaBH₄

4: LiAlH₄, AlCl₃ / tetrahydrofuran; diethyl ether

5: (i) BBr₃, CH₂Cl₂, (ii) aq. HBr, (iii) /BRN= 102415/, Et₂O, MeOH

With lithium aluminium tetrahydride; aluminium trichloride; trichlorophosphate; In tetrahydrofuran; diethyl ether; chloroform;

DOI:10.1248/cpb.25.1636

Reference yield:

(S)-72-benzoyl-34,76,7,92-tetramethoxy-71,2,3,4-tetrahydro-4,8-dioxa-12-aza-3(1,3),5,9(1,4)-tribenzena-7(1,8)-isoquinolina-tridecaphanedioic acid 13-tert-butyl ester 1-(4-nitro-phenyl) ester (64434-38-4) → 2-benzyl-6,7,6',12'-tetramethoxy-2'-methyl-(1'αH)-oxyacanthane (61897-96-9)

Guidance literature:

Multi-step reaction with 4 steps

1: (i) CF₃CO₂H, (ii) Py, DMF

2: POCl₃ / CHCl₃

3: (i) NaBH₄, MeOH, (ii) /BRN= 1209228/, (iii) NaBH₄

4: LiAlH₄, AlCl₃ / tetrahydrofuran; diethyl ether

With lithium aluminium tetrahydride; aluminium trichloride; trichlorophosphate; In tetrahydrofuran; diethyl ether; chloroform;

DOI:10.1248/cpb.25.1636

Downstream raw materials:

2-benzoyl-6,7,6',12'-tetramethoxy-1',17'-seco-oxyacanthan-1'-one

2-benzyl-7,6'-epoxy-6,12'-dimethoxy-2'-methyl-(1'αH)-oxyacanthane

2-benzyl-6,7,6',12'-tetramethoxy-2'-methyl-oxyacanthane

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