<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

Base Information

Chemical Name:<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.
CAS No.:80970-71-4
Molecular Formula:C₃₉H₅₈N₆O₂₀
Molecular Weight:930.918
Hs Code.:

<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

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Chemical Property of <6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

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Technology Process of <6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

There total 12 articles about <6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 70-34-8,65727-75-5
2,4-Dinitrofluorobenzene

: 80970-70-3
C₃₃H₅₆N₄O₁₆

: 80970-71-4
<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

Guidance literature:: With sodium hydrogencarbonate; In ethanol; water; for 12h;

Reference yield:

: 35905-31-8
Benzyl 2,3-anhydro-4,6-O-benzylidene-α-D-mannopyranoside

: 80970-71-4
<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

Guidance literature:: Multi-step reaction with 11 steps

1: 78 percent / NaN₃, NH₄Cl / 2-methoxy-ethanol; H₂O / 4 h / Heating

2: H₂ / 10percent Pd/C / methanol / 2 h

3: 0.5N HCl / H₂O / 10 h / Heating

4: 110 mg / Amberlite IRA 400 OH(-) / methanol; H₂O

5: 49 percent / methanol / 4 h / Heating

6: 0.55 mmol / H₂ / 10percent Pd/C / methanol / 2 h

7: 750 mg / ethanol / 5 h / Heating

8: H₂ / 10percent Pd/C / methanol / 2 h

9: 60 percent / ethanol; 2-methoxy-ethanol / 5 h / Heating

10: H₂ / 10percent Pd/C / methanol / 2 h

11: 56 percent / NaHCO₃ / ethanol; H₂O / 12 h

With hydrogenchloride; sodium azide; Amberlite IRA 400 OH(-); hydrogen; sodium hydrogencarbonate; ammonium chloride; palladium on activated charcoal; In methanol; ethanol; 2-methoxy-ethanol; water;

Reference yield:

: 80970-55-4
3-amino-1,6-anhydro-3-deoxy-β-D-altropyranose

: 80970-71-4
<6-<(1,6-Anhydro-3-desoxy-β-D-altropyranos-3-yl)amino>-3,6-didesoxy-1,2-O-isoprpyliden-α-D-glucofuranos-3-yl>-<3-<(3,6-didesoxy-3-(2,4-dinitroanilino)-1,2-O-isopropyliden-α-D-glucofuranos-6-yl)-amino>-3,6-didesoxy-1,2-O-isopropyliden-α-D-glucofur.>.

Guidance literature:: Multi-step reaction with 7 steps

1: 49 percent / methanol / 4 h / Heating

2: 0.55 mmol / H₂ / 10percent Pd/C / methanol / 2 h

3: 750 mg / ethanol / 5 h / Heating

4: H₂ / 10percent Pd/C / methanol / 2 h

5: 60 percent / ethanol; 2-methoxy-ethanol / 5 h / Heating

6: H₂ / 10percent Pd/C / methanol / 2 h

7: 56 percent / NaHCO₃ / ethanol; H₂O / 12 h

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; ethanol; 2-methoxy-ethanol; water;