Technology Process of C17H20N2O3
There total 7 articles about C17H20N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 100 percent / H2 / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr
2.1: 100 percent / 1 h / Heating
3.1: N-bromosuccinimide; benzoyl peroxide / CCl4 / 24 h / 10 °C / Irradiation
3.2: 1.39 g / dimethylformamide / 24 h / 20 °C
4.1: 96 percent / sodium methoxide / methanol / 3 h / 20 °C
5.1: 12 percent / AlH3 / tetrahydrofuran / 0.5 h / 20 °C
With
aluminium hydride; N-Bromosuccinimide; hydrogen; sodium methylate; dibenzoyl peroxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; tetrachloromethane;
DOI:10.1080/00397910701489537
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: 77 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride; 1-hydroxybenzotriazole; Et3N / dimethylformamide / 5 h / 20 °C
2.1: 100 percent / H2 / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr
3.1: 100 percent / 1 h / Heating
4.1: N-bromosuccinimide; benzoyl peroxide / CCl4 / 24 h / 10 °C / Irradiation
4.2: 1.39 g / dimethylformamide / 24 h / 20 °C
5.1: 96 percent / sodium methoxide / methanol / 3 h / 20 °C
6.1: 12 percent / AlH3 / tetrahydrofuran / 0.5 h / 20 °C
With
aluminium hydride; N-Bromosuccinimide; hydrogen; sodium methylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dibenzoyl peroxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1080/00397910701489537
