μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer

Base Information

Chemical Name:μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer
CAS No.:1227003-70-4
Molecular Formula:C₃₂H₅₈Cl₆N₄Si₂Zr₂
Molecular Weight:950.176
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer

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Technology Process of μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer

There total 1 articles about μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1227003-71-5
lithium μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidate dimer

: 10026-11-6
zirconium(IV) chloride

: 1227003-70-4
μ2,η1-N-[(N,N-dimethylamino)dimethylsilyl]-2,6-diisopropylanilidozirconium chloride dimer

Guidance literature:: In tetrahydrofuran; (Ar); std. Schlenk technique; HfCl4 (1 equiv.) was added to soln. of Li compd. (2 equiv.) in THF at -78°C; stirred while warmed to room temp.; stirred for 24 h; evapd. (vac.); extd. (toluene); filtered; dried (vac.); dissolved in CH2Cl2; crystd. at -10°C; elem. anal.;
DOI:10.1021/om100044b